How to remove oil from impregnated sintered metal?

Mar 17, 2005 3 Replies

Hi group, I have an element made of sintered metal, it has open pores and is impregnated with oil (kind of light machine oil). Prior to chemical analysis I need to remove that oil from pores. I've already tried boiling in acetone inside distilling column, it did a good thing to it, but not perfect. What solvent or a proverbal trick would you recommend to get rid of the oil. I dont have vacuum furnace, just simple distilling column. Was thinking about ether but safety and health issues scares me :). What about xylene or toluene? What will work better than acetone?



Thanks a lot!


..... What will work better than acetone?

Acetone is not a brilliant solvent for oils. We use Trichloroethylene or there is a solvent called SBP2 - used in oil labs for removing oils !

Steve

Try with Triclorethilene vapours ! Try in open space.

Xylene or toluene would be better. I would use a Soxlet extractor if you can get one. Frank

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